I am not an expert, however, after discussions with other who are experts, I can say one thing: measurements, particularly in the lower end of the frequency spectrum, are very difficult to perform, doing the experiments well and interpreting the results correctly require know how which is best acquired by doing a degree in a relevant field - I am not sure "give it up" is the only answer. However, if you are really interested in pursuing this to a correct result, and you have the resources, maybe engaging an acoustics consultant would be the right thing to to. Getting the measurements done, and simply paying for the extra service of "learning" the theory and practice from the guy who would do the measurements, so that you can continue, and fine tune. I thing it is a great thing that an audio enthusiast goes this far in an effort to bring in some exactness and precision to the "hifi" hobby, I suggest, do not give up.